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Ruthenium-catalyzed Oppenauer-type oxidation of 3 beta-hydroxy steroids. A highly efficient entry into the steroidal hormones with 4-en-3-one functionality
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- Almeida, MLS (author)
- Uppsala universitet
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- Kocovsky, P (author)
- Uppsala universitet
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- Backvall, JE (author)
- Uppsala universitet
- (creator_code:org_t)
- AMER CHEMICAL SOC, 1996
- English 6587-6590 s.
- In: JOURNAL OF ORGANIC CHEMISTRY. - : AMER CHEMICAL SOC. ; 61:19
- Other publication (other academic/artistic)
Abstract
Subject headings
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- Oxidation of 5-unsaturated 3 beta-hydroxy steroids 1 to the corresponding 4-en-3-one derivatives 2 can be performed efficiently by acetone at reflux in the presence of a catalytic system consisting of either (PPh(3))(3)RuCl2 (3) and K2CO3 or [(C(4)Ph(4)C
Keyword
- AEROBIC OXIDATION; SELECTIVE AROMATIZATION; A-RING; ALCOHOLS; FRAGMENT
Publication and Content Type
- vet (subject category)
- ovr (subject category)
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